By S. S. Labana
content material: Formation and houses of polymer networks : experimental and theoretical reviews / J.L. Stanford, R.F.T. Stepto, and R.H. nonetheless --
laptop simulation of end-linked elastomers : sol-gel distributions at excessive extents of response / Yu-Kwan Leung and B.E. Eichinger --
Rheological alterations throughout the copolymerization of vinyl and divinyl monomers / D.T. Landin and C.W. Macosko --
Elastomeric poly(dimethylsiloxane) networks with various short-chain segments / J.E. Mark and J.G. Curro --
gentle scattering of randomly cross-linked polystyrene / Kanji Kajiwara and Walther Burchard --
Correlation networks in polymeric fabrics decided via small-angle neutron scattering / L.H. Sperling, A.M. Fernandez, and G.D. Wignall --
Carboxyl-terminated butadiene-acrylonitrile-modified epoxy resin and its graphite fiber-reinforced composite : morphology and dynamic mechanical homes / Su-Don Hong, Shirley Y. Chung, George Neilson, and Robert F. Fedors --
Mechanical habit of a few epoxies with epoxidized usual oils as reactive diluents / Shahid Qureshi, J.A. Manson, J.C. Michel, R.W. Hertzberg, and L.H. Sperling --
quantity restoration in aerospace epoxy resins : results on time-dependent houses of carbon fiber-reinforced epoxy composites / Eric S.W. Kong --
constitution and fracture of hugely cross-linked networks / J.D. Lemay, B.J. Swetlin, and F.N. Kelley --
Fractographic impression of glassy natural networks / D.T. Turner --
Peroxide cross-linked ordinary rubber and cis-polybutadiene : characterization by way of high-resolution solid-state carbon-13 NMR / Dwight J. Patterson and Jack L. Koenig --
Carbon-13 magic perspective NMR spectroscopic reviews of an epoxy resin community / A. Cholli, W.M. Ritchey, and Jack L. Koenig --
NMR kinetic research of polyethylene-peroxide cross-linking reactions / V.D. McGinniss and J.R. Nixon --
Degradation chemistry of basic cross-links in high-solids tooth finishes : solar-assisted hydrolysis / Alan D. English and Harry J. Spinelli --
IR spectroscopic reviews of decay in cross-linked networks : photoenhanced hydrolysis of acrylic-melamine coatings / D.R. Bauer and L.M. Briggs --
Electron spin resonance (ESR) of photodegradation in polymer networks : photoinitiation expense size via nitroxide termination / John L. Gerlock, David R. Bauer, and L.M. Briggs --
hugely cross-linked CR-39 polycarbonate and its degradation by means of high-energy radiation / J.L. Cercena, J. Groeger, A.A. Mehta, R. Prottas, J.F. Johnson, and S.J. Huang.
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Additional resources for Characterization of Highly Cross-linked Polymers
ACS Symposium Series; American Chemical Society: Washington, DC, 1984. Vinyl and Divinyl Copolymerization LANDIN A N D MACOSKO 11 1 1 1 1 1 1 -ι 1 r- S 01 0 Figure 3. point. Conversion Qualitative trend of parameter s up to the gel 2E-5 (0 ça Concentration of D i v i n y l Figure 4. Cumulative rate of cyclization vs. i n i t i a l con centration of EGDMA. ; ACS Symposium Series; American Chemical Society: Washington, DC, 1984. 44 HIGHLY CROSS-LINKED POLYMERS 1E6 Figure 5. V i s c o s i t y v s .
Of course, we would eventually like to be able to relate prop erties to structure directly by using a suitable dynamic theory of polymers. Reptation theory (15) i s one which may be of great val ue for this purpose in the future. Below we report a simple way to include cyclization in branch ing theory and some i n i t i a l results for viscosity and conversion measurements on a nonlinear radical polymerization. We find a useful correlation between viscosity and C M L . w M t n e ) W Experimental The chemical system studied was that of the network forming copol ymer ization of methyl methacrylate (Aldrich) with small amounts of ethylene glycol dimethacrylate (Monomer Polymer Laboratories).
F. τ. Stepto, i n Developments in Polymerization- 3, Edited by R. N. Haward, Applied Science, Essex, England, Chpt. 3. Michael Falk and Ruth E. Thomas, Can. J. , 52, 3285 (1974). Josef Mikešand Karel Dušek, Macromolecules, 15, 93 (1982). B. E. Eichinger, J. Chem. , 75, 1964 (1981); Β. E. Eichinger and J . E. Martin, J. Chem. , 69, 4595 (1978). Y. K. Leung and Β. E. Eichinger, Preprint, Div. of Polym. , 48, ooo, (1983). (11) P. J . Flory, Statistical Mechanics of Chain Molecules, Interscience, New York, 1969.