Analytical Chemistry of Liquid Fuel Sources by Uden P.C., Siggia S., Jensen H.B. (eds.)

By Uden P.C., Siggia S., Jensen H.B. (eds.)

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ACS Symposium Series; American Chemical Society: Washington, DC, 1984. Vinyl and Divinyl Copolymerization LANDIN A N D MACOSKO 11 1 1 1 1 1 1 -ι 1 r- S 01 0 Figure 3. point. Conversion Qualitative trend of parameter s up to the gel 2E-5 (0 ça Concentration of D i v i n y l Figure 4. Cumulative rate of cyclization vs. i n i t i a l con­ centration of EGDMA. ; ACS Symposium Series; American Chemical Society: Washington, DC, 1984. 44 HIGHLY CROSS-LINKED POLYMERS 1E6 Figure 5. V i s c o s i t y v s .

Of course, we would eventually like to be able to relate prop­ erties to structure directly by using a suitable dynamic theory of polymers. Reptation theory (15) i s one which may be of great val­ ue for this purpose in the future. Below we report a simple way to include cyclization in branch­ ing theory and some i n i t i a l results for viscosity and conversion measurements on a nonlinear radical polymerization. We find a useful correlation between viscosity and C M L . w M t n e ) W Experimental The chemical system studied was that of the network forming copol­ ymer ization of methyl methacrylate (Aldrich) with small amounts of ethylene glycol dimethacrylate (Monomer Polymer Laboratories).

F. τ. Stepto, i n Developments in Polymerization- 3, Edited by R. N. Haward, Applied Science, Essex, England, Chpt. 3. Michael Falk and Ruth E. Thomas, Can. J. , 52, 3285 (1974). Josef Mikešand Karel Dušek, Macromolecules, 15, 93 (1982). B. E. Eichinger, J. Chem. , 75, 1964 (1981); Β. E. Eichinger and J . E. Martin, J. Chem. , 69, 4595 (1978). Y. K. Leung and Β. E. Eichinger, Preprint, Div. of Polym. , 48, ooo, (1983). (11) P. J . Flory, Statistical Mechanics of Chain Molecules, Interscience, New York, 1969.

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