By Uden P.C., Siggia S., Jensen H.B. (eds.)
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ACS Symposium Series; American Chemical Society: Washington, DC, 1984. Vinyl and Divinyl Copolymerization LANDIN A N D MACOSKO 11 1 1 1 1 1 1 -ι 1 r- S 01 0 Figure 3. point. Conversion Qualitative trend of parameter s up to the gel 2E-5 (0 ça Concentration of D i v i n y l Figure 4. Cumulative rate of cyclization vs. i n i t i a l con centration of EGDMA. ; ACS Symposium Series; American Chemical Society: Washington, DC, 1984. 44 HIGHLY CROSS-LINKED POLYMERS 1E6 Figure 5. V i s c o s i t y v s .
Of course, we would eventually like to be able to relate prop erties to structure directly by using a suitable dynamic theory of polymers. Reptation theory (15) i s one which may be of great val ue for this purpose in the future. Below we report a simple way to include cyclization in branch ing theory and some i n i t i a l results for viscosity and conversion measurements on a nonlinear radical polymerization. We find a useful correlation between viscosity and C M L . w M t n e ) W Experimental The chemical system studied was that of the network forming copol ymer ization of methyl methacrylate (Aldrich) with small amounts of ethylene glycol dimethacrylate (Monomer Polymer Laboratories).
F. τ. Stepto, i n Developments in Polymerization- 3, Edited by R. N. Haward, Applied Science, Essex, England, Chpt. 3. Michael Falk and Ruth E. Thomas, Can. J. , 52, 3285 (1974). Josef Mikešand Karel Dušek, Macromolecules, 15, 93 (1982). B. E. Eichinger, J. Chem. , 75, 1964 (1981); Β. E. Eichinger and J . E. Martin, J. Chem. , 69, 4595 (1978). Y. K. Leung and Β. E. Eichinger, Preprint, Div. of Polym. , 48, ooo, (1983). (11) P. J . Flory, Statistical Mechanics of Chain Molecules, Interscience, New York, 1969.